The Development of a Sapphire Cell for Neutron Scattering Experiments at High Temperature and High Pressure [electronic resource]

Abstract. A high pressure, high temperature sapphire cell has been designed to provide users at the Spallation Neutron Source with the ability to perform in-situ supercritical bulk water studies. The design criteria for the cell required the achievement of a maximum pressure of 150 MPa at the maximu...

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Bibliographic Details
Online Access: Online Access
Corporate Authors: Oak Ridge National Laboratory (Researcher), Oak Ridge National Laboratory. Spallation Neutron Source (Researcher)
Format: Government Document Electronic eBook
Language:English
Published: Washington, D.C. : Oak Ridge, Tenn. : United States. Dept. of Energy. Office of Science ; distributed by the Office of Scientific and Technical Information, U.S. Dept. of Energy, 2010.
Subjects:

MARC

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500 |a International Conference on Neutron Scattering (ICNS) 2009, Knoxville, TN, USA, 20090503, 20090503. 
500 |a Luttrell, Claire Roberta; Walker, Lakeisha MH; Solomon, Landon M; Church, Andrew J. 
520 3 |a Abstract. A high pressure, high temperature sapphire cell has been designed to provide users at the Spallation Neutron Source with the ability to perform in-situ supercritical bulk water studies. The design criteria for the cell required the achievement of a maximum pressure of 150 MPa at the maximum temperature of 500 C. Other conceptual constraints, such as a 360 viewing angle and top loading integration further complicated and limited available cell models. The sapphire cell was tested and modified due to pre-mature failure. Due to convenient geometry and ease of operation, interest in the cell for more moderate operating requirements has increased. 
536 |b DE-AC05-00OR22725. 
650 7 |a Design.  |2 local. 
650 7 |a Water.  |2 local. 
650 7 |a Scattering.  |2 local. 
650 7 |a Pressure Range Mega Pa 100-1000.  |2 local. 
650 7 |a Neutron Sources.  |2 local. 
650 7 |a Geometry.  |2 local. 
650 7 |a Temperature Range 0400-1000 K.  |2 local. 
650 7 |a Neutron Diffraction.  |2 local. 
650 7 |a Spallation.  |2 local. 
650 7 |a Sapphire.  |2 local. 
650 7 |a Physics Of Elementary Particles And Fields.  |2 edbsc. 
710 2 |a Oak Ridge National Laboratory.  |4 res. 
710 2 |a Oak Ridge National Laboratory.  |b Spallation Neutron Source.  |4 res. 
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